5H-Pyrrolo[3,4-b]pyridine, 6,7-dihydro-, dihydrochloride
6,7-Dihydro-5H-pyrrolo[3,4-b]pyridine dihydrochloride
CAS: 147740-02-1
Molecular Formula: C7H9ClN2
5H-Pyrrolo[3,4-b]pyridine, 6,7-dihydro-, dihydrochloride - Names and Identifiers
5H-Pyrrolo[3,4-b]pyridine, 6,7-dihydro-, dihydrochloride - Physico-chemical Properties
| Molecular Formula | C7H9ClN2 |
| Molar Mass | 156.61276 |
| Boling Point | 288.9℃ at 760mmHg |
| Storage Condition | under inert gas (nitrogen or Argon) at 2-8°C |
| MDL | MFCD09607967 |
5H-Pyrrolo[3,4-b]pyridine, 6,7-dihydro-, dihydrochloride - Reference Information
| application | 6, 7-dihydro-5H-pyrrole [3,4-b] pyridine hydrochloride can be used as an organic synthesis intermediate and pharmaceutical intermediate, mainly used in laboratory research and development process and chemical and pharmaceutical production process. |
| Preparation | Add 6-(2, 4-dimethoxybenzyl)-6, 7-dihydro-5H-pyrrolo [3,4-b] pyridine (34.9 mmol) in a dry flask under nitrogen. Trifluoroacetic acid (27 ml) and triethylsilane (6.0 ml) were added to the reaction mixture. Stir the reaction mixture. Heat the reaction mixture at 60°C for 5 hours. Vacuum removes volatiles to obtain viscous oil. Add HCl to the residue (4 M in dioxane, 40 ml), then add ethyl acetate (50 ml). The reaction mixture was vigorously stirred for about 1 hour at room temperature to provide precipitation. The solids are separated by filtration. The solids were washed with ethyl acetate (25ml). Vacuum drying of solids. |
Last Update：2024-04-09 15:16:39
![5H-Pyrrolo[3,4-b]pyridine, 6,7-dihydro-, dihydrochloride](http://res.chembk.com/assets/images/structure/147740-02-1.gif)
Supplier List
Product Name: 6,7-Dihydro-5H-pyrrolo[3,4-b]pyridine dihydrochloride Visit Supplier Webpage Request for quotation
CAS: 147740-02-1
Tel: 18301782025
Email: 3008007409@qq.com
Mobile: 18021002903
QQ: 3008007409
Wechat: 18301782025
CAS: 147740-02-1
Tel: 18301782025
Email: 3008007409@qq.com
Mobile: 18021002903
QQ: 3008007409
Wechat: 18301782025
Product Name: 6,7-Dihydro-5H-pyrrolo[3,4-b]pyridine dihydrochloride Visit Supplier Webpage Request for quotation
CAS: 147740-02-1
Tel: 18301782025
Email: 3008007409@qq.com
Mobile: 18021002903
QQ: 3008007409
Wechat: 18301782025
CAS: 147740-02-1
Tel: 18301782025
Email: 3008007409@qq.com
Mobile: 18021002903
QQ: 3008007409
Wechat: 18301782025
View History